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Laboratory Reactor: Proper Installation and Use of Laboratory Reactors
In the laboratory, the laboratory reactor is a commonly used piece of equipment for conducting reactions involving various chemical substances. It operates smoothly, is easy to use, and produces little noise. Below, we’ll outline several key points to keep in mind during its installation. 1. Installation Location: The reactor should be installed in a high-pressure operating room that meets explosion-proof requirements. When multiple reaction vessels are installed, they should be placed separately, with each pair of reactors separated by a safe, explosion-proof wall. Each operating room must have an outdoor passageway and an emergency exit. If explosive media are present, the equipment must be well-ventilated.
Release time:
2021-04-16 09:24
Source:
In the laboratory, Laboratory Reactor This is a common piece of equipment used by companies that analyze reactions involving various chemical substances. It operates smoothly, is easy to use, and produces no noise. Next, let’s discuss several key points to keep in mind during installation.
1. Installation Location: The equipment should be installed in a high-voltage operating room that meets explosion-proof requirements. When multiple reaction vessels are installed, they should be placed separately, with each pair of reactors separated by a safe, explosion-proof wall. Each operating room must have an outdoor passageway and an exit. When explosive media are present, the equipment must be well-ventilated.
2. After opening the package, check whether the equipment is damaged. Install the equipment according to the structural diagram, based on its model. Verify that all spare parts are included by checking against the packing list.
3. Laboratory Reactor Cleaning After each operation, clean the reactor body and sealing surfaces with a cleaning solution. Clean regularly to keep them clean. Do not use hard materials or rough surfaces for cleaning.
4. Laboratory Reactor Installation and Sealing of the Reactor Body and Reactor Lid The vessel body and lid are sealed with stainless steel spiral gaskets. Tighten the main nut gradually and symmetrically, applying even pressure to achieve a good seal. When tightening the nut, ensure that the tightening is done diagonally and symmetrically, with uniform force; otherwise, the lid may tilt to one side, compromising the sealing performance.
5. Both the feeding tank and the condenser must be operable under vacuum conditions. When the reaction process generates pressure, the needle valves connected to the feeding tank and the condensation system should be closed to prevent excessive working pressure from damaging the glass level gauge, the feeding tank, and the condenser, thus avoiding serious hazards.
6. Installation of valves, connecting fittings, safety valves, and temperature-sensing protection tubes: Use tightening to achieve a sealing effect. The arc-shaped sealing surfaces at both ends of the joints must not be allowed to rotate relative to each other. All threaded connections should be assembled using graphite mixed with lubricating oil or grease to prevent them from becoming difficult to disassemble in the future.
In addition, after the equipment is installed, a certain amount of nitrogen pressure is introduced. In 30 minutes, check for any leaks. If a leak is detected, use soap bubbles to pinpoint the exact location of the leak. After identifying and sealing the leak, reapply nitrogen pressure for another test to ensure there are no further leaks before starting normal operation. Laboratory Reactor Before starting, the cooling water in the jacket between the magnetic stirrer and the kettle lid needs to be checked to ensure that the water temperature is below. 35 degrees Celsius, to avoid high-magnetic substances.
Weihai Automatic Control Reactor Co., Ltd. is a manufacturer. Magnetic Stirred Reactor 、 Hydrogenation Reactor 、 Laboratory Reactor 、 Stainless Steel Reactor of the Reaction vessel Manufacturers, you're welcome to come and discuss cooperation!
Laboratory reactor, hydrogenation reactor, hydriding reactor
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